Hydracrylonitrile → HCID 86744987, compound

Participants

Reaction Steps

0.68 ml (10 mmol) of 2-cyanoethanol are reacted analogously to Example 2 with 2 ml (11 mmol) of phosphorous acid methyl ester-diisopropylamide-chloride in the presence of 8 ml of diisopropylethylamine in 20 ml of freshly distilled methylene chloride. Drying at 30° C. in a high vacuum gives 2.5 g of an oil which, according to 31P-NMR, contains 94% of the compound VIII. ##STR15##

Provenance & Evidence