HCID 19996463, compound → HCID 19996380, compound

Participants

Reaction Steps

807 mg of N-[3-[6-(1-t-butoxyformamido)hexanamido]-5-nitrobenzoyl]-β-alanine are left to stand at room temperature in 2.7 ml of formic acid for 18 hours. The solvent is evaporated in a vacuum. The residue is dissolved in water and the solution is evaporated in a vacuum. There are obtained 573 mg of N-[3-(6-aminohexanamido)-5-nitrobenzoyl]-β-alanine formate (2:1), MS: 367 (67, M+H).

Provenance & Evidence