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HRID2248498

反应详情

EQUATION

反应方程式

HRID 2248498 的结构方程式

REACTANTS

反应物

3
结构：CC(C)(C)OC(=O)NCCC(=O)O
HCID76809

N-((1,1-Dimethylethoxy)carbonyl)-beta-alanine

C8H15NO4

结构：Nc1ccc([N+](=O)[O-])c(C(=O)O)c1
HCID83298

5-Amino-2-nitrobenzoic acid

C7H6N2O4

结构：CC(C)(C)OC(=O)CCNC(=O)c1cc(NC(=O)CCNC(=O)OC(C)(C)C)ccc1[N+](=O)[O-]
HCID19996354

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)NCCC(=O)Nc1ccc([N+](=O)[O-])c(C(=O)O)c1
HCID54030903

未命名化合物

PROCEDURE

实验过程

For the preparation of the ester starting material, N-(t-butoxycarbonyl)-β-alanine and 5-amino-2-nitrobenzoic acid are coupled to give 5-[3-(1-t-butoxyformamido)propionamido]-2-nitrobenzoic acid, MS: 354 (17, M+H), and the latter is reacted with β-alanine t-butyl ester.