HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Aminobenzoic Acid → HCID 53962591, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Aminobenzoic Acid | HCID 7419 | — |
| Reactant | 5-(((Tert-butoxy)carbonyl)amino)pentanoic acid | HCID 545848 | — |
| Product | HCID 53962591 | HCID 53962591 | — |
Reaction Steps
5-[1-(t-Butoxy)formamido]valeric acid is coupled with m-aminobenzoic acid to give m-[5-(1-t-butoxyformamido)valeramido]benzoic acid, m.p. 188° C., and the latter is reacted with 3-amino-3-phenylpropionic acid benzyl ester p-toluenesulphonate to give DL-N-[m-[5-(1-t-butoxyformamido)valeramido]benzoyl]-3-phenyl-β-alanine benzyl ester, MS: 574 (17, M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05039805 |
| Source dataset | uspto-grants-1991_08 |
| ORD ID | ord-28a7302f45174a3c83169d137bc80712 |
| Source note | uspto-grants-1991_08 |