Sodium Acetate → HCID 10405634, compound

Participants

Reaction Steps

3.4 g of product obtained in stage A are heated to reflux for 1 hour with 3.4 g of sodium acetate in 68 cm3 of acetic anhydride. The mixture is cooled to room temperature and evaporated to dryness, the residue is taken up in 50 cm3 of water, filtered off and dried and 2.87 g of expected product are obtained. M.p. 150°-152° C. After crystallization in isopropanol, 1.9 g of pure product are obtained. M.p. 152°-153° C.

Provenance & Evidence