HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3,3-bis(methoxycarbonyl methylthio)-2-methyl-propionate → Methyl 3-hydroxy-4-methylthiophene-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3,3-bis(methoxycarbonyl methylthio)-2-methyl-propionate | HCID 19995022 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Sodium Methoxide | HCID 10942334 | — |
| Product | Methyl 3-hydroxy-4-methylthiophene-2-carboxylate | HCID 54710749 | — |
Reaction Steps
Dithioacetal of (b) above (0.08 mol) was dissolved in 120 ml of 2N sodium methoxide in methanol and stirred over night at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05041461 |
| Source dataset | uspto-grants-1991_08 |
| ORD ID | ord-910e94acaeac4f238276630e81ad0697 |
| Source note | uspto-grants-1991_08 |