HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → Methyl 2-chloro-4-methyl-3-oxo-2,3-dihydrothiophene-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | Thiophen-2-ol | HCID 10909502 | — |
| Reactant | Methyl 3-hydroxy-4-methylthiophene-2-carboxylate | HCID 54710749 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | Methyl 2-chloro-4-methyl-3-oxo-2,3-dihydrothiophene-2-carboxylate | HCID 14642334 | — |
Reaction Steps
N-Chlorosuccinimide (0.027 mol) was added to a stirred solution of the hydroxythiophen of (c) above (3 g) in 8 ml of carbon tetrachloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05041461 |
| Source dataset | uspto-grants-1991_08 |
| ORD ID | ord-13794088a2884ec4a4c8159d16c9ab53 |
| Source note | uspto-grants-1991_08 |