HCID 15162481, compound → HCID 15162482, compound

Participants

Reaction Steps

To a 45 mL Hastelloy "C" pressure reactor was added 4.5 g of 2,6-difluoro-3,4,5-trichloronitrobenzene, 0.91 g of 10 percent palladium on charcoal and 25 mL of iso-propyl alcohol. The reactor was purged with nitrogen, sealed and pressurized to 130 psig with hydrogen. After stirring at ambient temperature for 5 hrs, the reactor was vented. The catalyst was removed by filtration and the solvent was evaporated under reduced pressure to give 3.7 g of solid product having a mp 137°-140° C. The IR, Mass and NMR spectra were consistent with the structure.

Provenance & Evidence