HCID 19995563, compound → HCID 19995551, compound

Participants

Reaction Steps

α,α-Diethoxymethyl-β-nitro-3,5-dimethoxybenzenepropanol (3.39 g) was hydrogenated in isoproipanol (50 ml) over Raney nickel at atmospheric pressure and room temperature. When hydrogen absorption was complete, the reaction mixture was degased for 15 minutes under vacuum and the catalyst was filtered on celite. The solvent was evaporated under vacuum to yield the title compound as an oil (2.38 g).

Provenance & Evidence