HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyethylamine → HCID 135856767, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyethylamine | HCID 8018 | — |
| Reactant | 4-Ethoxy-3-(5-methyl-4-oxo-7-propyl-1,4-dihydroimidazo[5,1-f][1,2,4]triazin-2-yl)benzene-1-sulfonyl chloride | HCID 135430159 | — |
| Reactant | HCID 136355239 | HCID 136355239 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 135856767 | HCID 135856767 | — |
Reaction Steps
By the same method, starting with 1.23 g (3 mmol) of 4-ethoxy-3-(5-methyl-4-oxo-7-propyl-3,4-dihydro-imidazo[5,1-f][1,2,4]triazin-2-yl)-benzenesulphonyl chloride and 680 mg (9 mmol) of 2-methoxyethylamine, 900 mg (67%) of N-(2-methoxyethyl)-3-(5-methyl-4-oxo-7-propyl-3,4-dihydro-imidazo[5,1-f][1,2,4]triazin-2-yl)-4-benzenesulphonamide are obtained. Rf=0.25 (dichloromethane/methanol=95:5)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07314871B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-fb4c39d6254a4688b5e1e4880808339b |
| Source note | uspto-grants-2008_01 |