HCID 11568876, compound → HCID 58670130, compound

Participants

Reaction Steps

To a solution of 2A (96 mg, 0.207 mmol) in THF (6 mL) and MeOH (6 mL) at RT was added palladium 5% wt on activated carbon (64 mg). The reaction mixture was stirred under a hydrogen balloon for 1 h. The reaction was filtered and the filtrate concentrated to give the title compound as a foam (68 mg, 100%). LC/MS (method A): retention time=2.65 min, (M+H)+=330.

Provenance & Evidence