HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 11356158, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Methyl 6-Bromohexanoate | HCID 4170292 | — |
| Reactant | Potassium cyanate | HCID 11378442 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 11356158 | HCID 11356158 | 77% |
Reaction Steps
The reaction of 10.45 grams of 6-bromohexanoic acid methyl ester with 6.08 grams of potassium cyanate and 2.7 grams of methanol in 50 ml DMF following the procedure of Example 1 gave 7.82 grams (76.9%) of 6-methoxycarbonylaminohexanoic acid methyl ester having a boiling point of 104° C./0.0013 mbar.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04234744 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-d650cda4d36044df91bdf1a415ecc60b |
| Source note | uspto-grants-1980_11 |