HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 70288-74-3
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Methyl 2-bromopropionate | HCID 95576 | — |
| Reactant | Potassium cyanate | HCID 11378442 | — |
| Product | 70288-74-3 | HCID 6421864 | 59% |
Reaction Steps
From the reaction of 11.69 grams of 2-bromopropionic acid methyl ester with 8.52 grams of potassium cyanate and 7.85 grams of methanol under the conditions described in Example 1 there were isolated 6.66 grams (59%) of 2-methoxycarbonylaminopropionic acid methyl ester with a boiling point of 65°-67° C./0.0013 mbar.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04234744 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-17b1c62716884293a7f30fb49e02d387 |
| Source note | uspto-grants-1980_11 |