HRID224957

反应详情

EQUATION

反应方程式

HRID 224957 的结构方程式

PROCEDURE

实验过程

14.64 grams of 2-bromo-4-methyl valeric acid methyl ester were brought to reaction with potassium cyanate and methanol in the manner described in Example 1 (using the same amounts of potassium cyanate and methanol as in Example 1 ), reaction time 1 hour and then worked up. There were obtained 9.39 grams (66%) of 2-methoxycarbonylamino-4-methyl valeric acid methyl ester with a boiling point of 100° C./0.0013 mbar.

WORKUP

后处理

  1. customreaction time 1 hour