HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 2-Methoxycarbonylamino-4-methyl valeric acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Potassium cyanate | HCID 11378442 | — |
| Reactant | Methyl 2-bromo-4-methylpentanoate | HCID 12957039 | — |
| Product | 2-Methoxycarbonylamino-4-methyl valeric acid methyl ester | HCID 14036586 | 66% |
Reaction Steps
14.64 grams of 2-bromo-4-methyl valeric acid methyl ester were brought to reaction with potassium cyanate and methanol in the manner described in Example 1 (using the same amounts of potassium cyanate and methanol as in Example 1 ), reaction time 1 hour and then worked up. There were obtained 9.39 grams (66%) of 2-methoxycarbonylamino-4-methyl valeric acid methyl ester with a boiling point of 100° C./0.0013 mbar.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04234744 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-f37da4faf31f4a6f901ba290ca6bfca5 |
| Source note | uspto-grants-1980_11 |