HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 14133519, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Methyl bromoacetate | HCID 60984 | — |
| Reactant | Potassium cyanate | HCID 11378442 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 14133519 | HCID 14133519 | 64.3% |
Reaction Steps
10.71 grams of monobromo acetic acid methyl ester, 8.52 grams of potassium cyanate and 7.85 grams of methanol were heated in 70 ml of DMF following the procedure of Example 1 gave 6.62 grams (64.3%) of methoxycarbonylamino acetic acid methyl ester having a boiling point of 67°-8° C./0.0013 mbar.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04234744 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-05549a776bd743fbaa64dcd7bca35360 |
| Source note | uspto-grants-1980_11 |