HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178512644, compound → HCID 178503912, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178512644 | HCID 178512644 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178503912 | HCID 178503912 | — |
Reaction Steps
To a solution of 2-guanidino-4-(4-aminobutyl)thiazole (0.8 g.) in ethanol (10 ml.) was added dimethyl (cyanoimido)dithiocarbonate (0.6 g.). The mixture was stirred overnight. The white precipitate was filtered off and recrystallized from acetonitrile to give 2-guanidino-4-[4-(3-cyano-2-methylisothioureido)butyl]thiazole, m.p. 178°-180° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04234735 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-f97b27b968ba4074b7d0e85b6e9c03c4 |
| Source note | uspto-grants-1980_11 |