HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Methylsulphonyl)-2-oxoimidazolidine-1-carbonyl chloride → HCID 53644563, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Methylsulphonyl)-2-oxoimidazolidine-1-carbonyl chloride | HCID 3016299 | — |
| Reactant | HCID 86737352 | HCID 86737352 | — |
| Solvent | Oxolane--water (1/1) | HCID 21881883 | — |
| Product | HCID 53644563 | HCID 53644563 | — |
Reaction Steps
The compound is prepared analogously to Example 6 (a) from 15 g of α-amino-α-(2-benzyloxycarbonylamino-thiazol-4-yl)-acetic acid dihydrate in THF/water (1:1) and 10.9 g 1-chlorocarbonyl-2-oxo-3-methylsulfonyl-imidazolidine in a pH-range from 7.5 to 8.0. 14.1 g (65% of theory) are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04235774 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-0907125cb33443f5a9cd4061126fd020 |
| Source note | uspto-grants-1980_11 |