HRID225036

反应详情

EQUATION

反应方程式

HRID 225036 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A suspension prepared from 55.0 g of granulated stearic acid (An 198, titer 66° C., particle size 100-300μ) and 8.1 g lithium hydroxide monohydrate in 550 ml of water is heated to 80° C. within 10-15 minutes. The remaining free fatty acid at this point is only 12.1%. Stirring is continued at 80° C. for the duration of one more hour and the resultant hollow granulate, which now contains only 0.4% free fatty acid, is filtered and dried.

WORKUP

后处理

  1. customtiter 66° C.
  2. customis continued at 80° C. for the duration of one more hour
  3. filtrationis filtered
  4. customdried