HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxylamine → HCID 178510916, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxylamine | HCID 787 | — |
| Reactant | 3-(4-Chlorophenyl)prop-2-enenitrile | HCID 34243 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178510916 | HCID 178510916 | 51% |
Reaction Steps
A solution of 3-(4-chloro-phenyl)-acrylonitrile (1.63 g, 10 mmol) and hydroxyamine (0.74 ml, 12 mmol) in ethanol (10 ml) was stirred at room temperature overnight. The solvent was evaporated, and the residue was purified by column chromatography (EtOAc:Hexane=1:3) to give 1.0 g (51%) of 3-(4-chloro-phenyl)-N-hydroxy-acrylamidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07317029B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-f73876dd3cff47bbb2dd0e877d4a4cee |
| Source note | uspto-grants-2008_01 |