HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → HCID 22139857, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | HCID 22139822 | HCID 22139822 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 22139857 | HCID 22139857 | 74.3% |
Reaction Steps
To (4-chloro-thiophen-3-yl)-(5,6-difluoro-1H-benzoimidazol-2-yl)-amine (125 mg) in acetic acid (8 ml) a solution of N-chlorosuccinimide (59 mg) in acetic acid (2 ml) was added. Following the analogous description in example 54c) the desired product (58 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07317033B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-be4edbd377a64ea5a2bf8d9668f75616 |
| Source note | uspto-grants-2008_01 |