HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 24824335, compound → HCID 19899911, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 24824335 | HCID 24824335 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 19899911 | HCID 19899911 | 69.1% |
Reaction Steps
2-(2-Fluoro-6-nitro-phenyl)-malonic acid dimethyl ester (6.5 g, 23.98 mmol) was refluxed in 200 mL 6N hydrochloric acid for 24 hours. The solid was collected by suction filtration, and dried to give 3.3 g, 54% yield of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07317037B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-6b0ef12fefc14dceb7776f77edad437a |
| Source note | uspto-grants-2008_01 |