HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methylthiophene-2-carbonyl chloride → 5-Methyl-thiophene-2-carboxylic acid [7-(3-dimethylamino-pyrrolidin-1-yl)-4-methoxy-benzothiazol-2-yl]-amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methylthiophene-2-carbonyl chloride | HCID 2760083 | — |
| Reactant | 7-(3-Dimethylamino-pyrrolidin-1-yl)-4-methoxy-benzothiazol-2-yl-amine | HCID 22283097 | — |
| Product | 5-Methyl-thiophene-2-carboxylic acid [7-(3-dimethylamino-pyrrolidin-1-yl)-4-methoxy-benzothiazol-2-yl]-amide | HCID 86584914 | — |
Reaction Steps
Using 5-methyl-thiophene-2-carbonyl chloride and 7-(3-dimethylamino-pyrrolidin-1-yl)-4-methoxy-benzothiazol-2-yl-amine the title compound was prepared using the general method of example 1 as yellow solid (90%), MS: m/e=417 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07317007B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-de4c3468b3cd4bb78707cdff8bb6c1ae |
| Source note | uspto-grants-2008_01 |