HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 18623111, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 23435349 | HCID 23435349 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18623111 | HCID 18623111 | — |
Reaction Steps
10 g of the hydrochloride of 1-formyl-4-[hydrazino(methylimino)methyl]piperazine are dissolved in 250 ml of methanol. 50 ml of HClconc. are added, the mixture obtained is stirred overnight and the solvent is evaporated. A solid residue is obtained which is dried over solid KOH. The trihydrochloride of 1-[hydrazino-(methylimino)methyl]piperazine is obtained in form of a white product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07317101B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-7959d66fd3fc4bb1981aaab150484ece |
| Source note | uspto-grants-2008_01 |