HRID2251134

反应详情

EQUATION

反应方程式

HRID 2251134 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

8-[4-(Tetrahydro-pyran-2-yloxy)-phenyl]-5H,7H-6-oxa-1,4,8a-triaza-s-indacene (500 mg, 2.5 mmol) was suspended in methanol and added with p-toluenesulfonic acid (50 mg) was catalyst. The mixture was stirred at room temperature for 2 hours and concentrated in vacuo. The residue was carried on to the next reaction without purification.

WORKUP

后处理

  1. concentrationconcentrated in vacuo
  2. customThe residue was carried on to the next reaction without purification