Hydrochloric Acid → HCID 69039147, compound

HRID 2251209Notes

Reaction equation

HRID 2251209 reaction equation
C(OC([N:8]1[CH2:13][CH2:12][N:11]([C:14]2[CH:19]=[N:18][C:17]([C:20](=[O:22])[NH2:21])=[CH:16][N:15]=2)[CH2:10][CH2:9]1)=O)(C)(C)C.[ClH:23]>O1CCOCC1>[ClH:23].[N:11]1([C:14]2[CH:19]=[N:18][C:17]([C:20]([NH2:21])=[O:22])=[CH:16][N:15]=2)[CH2:12][CH2:13][NH:8][CH2:9][CH2:10]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 69039443HCID 69039443, compound

Product 1

HCID 69039147HCID 69039147, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

0.25 mmol of 5′-Carbamoyl-2,3,5,6-tetrahydro-[1,2′]bipyrazinyl-4-carboxylic acid tert-butyl ester was stirred for 1 hour in 1 ml of dioxane saturated with gaseous HCl. Concentration of the reaction mixture led to the title compound, as a colorless solid. MS (m/e): 208.3 (MH+, 100%)

Sources & evidence

ORD record
ord-9a549db150be4df8b7c2443a952ced7e
Source dataset
uspto-grants-2008_01
Patent number
US07319099B2

Reaction notes

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