HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 69039149, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 69038776 | HCID 69038776 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 69039149 | HCID 69039149 | — |
Reaction Steps
4-(5-Trifluoromethyl-pyridazin-3-yl)-piperazine-1-carboxylic acid tert-butyl ester (45 mg) was dissolved in dichloromethane (0.5 mL), and trifluoroacetic acid was added (0.5 mL). The reaction mixture was stirred for 30 minutes before being concentrated in vacuo to afford the crude title compound which was used directly in the next step without further purification or analysis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07319099B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-28c111e68f6f4b4d821fe8ba6f3850cc |
| Source note | uspto-grants-2008_01 |