HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2251304Generated: November 2, 2026
Potassium Carbonate → HCID 59643624, compound
https://huagongshe.com/reaction/2251304
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Fluorobenzyl bromide | HCID 68021 | — |
| Reactant | HCID 68574706 | HCID 68574706 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 59643624 | HCID 59643624 | — |
Reaction Steps
4-Fluorobenzyl bromide (18.9 mg) and potassium carbonate (27.6 mg) were added to a mixture of {3-[4-(3-dimethylaminopyrrolidin-1-yl)phenyl][1,2,4]oxadiazol-5-yl}methanol (28.8 mg) and DMF (0.3 ml). The reaction mixture was stirred at 60° C. for 3 h, filtered and purified by preparative HPLC. The product with the molecular weight of 396.20 (C22H25FN4O2) was obtained in this way; MS (ESI): 397.27 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07319108B2 |
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| Source dataset | uspto-grants-2008_01 |
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| ORD ID | ord-740bffd8302248cc99fd09b89a5da476 |
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| Source note | uspto-grants-2008_01 |
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