HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 23329184, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 12199686 | HCID 12199686 | — |
| Product | HCID 23329184 | HCID 23329184 | — |
Reaction Steps
A solution of 10 g of 3-methyl-3-azabicyclo[3.1.0]-hexane-1-carbonitrile is 60 ml of saturated ethanolic KOH and 20 ml of water is boiled under reflux for 15 hours. After neutralization with hydrochloric acid the mixture is evaporated and the title compound is extracted from the resultant dried residue with hot absolute ethanol (M.P. 193°-195°).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04235921 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-1f7c16e7d879450b9f9cf03cf27fb9d0 |
| Source note | uspto-grants-1980_11 |