HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 59643371, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 59643333 | HCID 59643333 | — |
| Product | HCID 59643371 | HCID 59643371 | 52% |
Reaction Steps
Hydrolysis of ethyl 2-[4-(2-{(5-bromopyridin-2-yl)[4-(trifluoromethyl)benzyl]amino}ethyl)phenoxy]-2-methylpropanoate with NaOH as per general procedure H provided after chromatography and crystallization from dichloromethane-hexane, the title compound as a white solid (56 mg; 52% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07319104B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-2e68b701ba11426fbf68ad01f6938a64 |
| Source note | uspto-grants-2008_01 |