Allyltributylstannane → HCID 59643197, compound

HRID 2251529Notes

Reaction equation

Br[C:2]1[CH:3]=[CH:4][C:5]([N:8]([CH2:26][C:27]2[CH:32]=[CH:31][C:30]([O:33][C:34]([F:37])([F:36])[F:35])=[CH:29][CH:28]=2)[CH2:9][CH2:10][C:11]2[CH:25]=[CH:24][C:14]([O:15][C:16]([CH3:23])([CH3:22])[C:17]([O:19]CC)=[O:18])=[CH:13][CH:12]=2)=[N:6][CH:7]=1.[CH2:38]([Sn](CCCC)(CCCC)CCCC)[CH:39]=[CH2:40]>>[CH3:22][C:16]([O:15][C:14]1[CH:13]=[CH:12][C:11]([CH2:10][CH2:9][N:8]([C:5]2[CH:4]=[CH:3][C:2]([CH2:38][CH2:39][CH3:40])=[CH:7][N:6]=2)[CH2:26][C:27]2[CH:32]=[CH:31][C:30]([O:33][C:34]([F:35])([F:36])[F:37])=[CH:29][CH:28]=2)=[CH:25][CH:24]=1)([CH3:23])[C:17]([OH:19])=[O:18]

Participants

Reactant 2

HCID 90628Allyltributylstannane

HCID 59643326HCID 59643326, compound

Product 1

HCID 59643197HCID 59643197, compound

Procedure

Similarly prepared from ethyl 2-[4-(2-{(5-bromopyridin-2-yl)[4-(trifluoromethoxy)benzyl]amino}ethyl)phenoxy]-2-methylpropanoate and allyltributyltin.

Sources & evidence

ORD record: ord-0918543130244a7faf0cb13144d4a701
Source dataset: uspto-grants-2008_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07319104B2

Reaction notes

Loading…