HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59643063, compound → HCID 59643052, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59643063 | HCID 59643063 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59643052 | HCID 59643052 | — |
Reaction Steps
To a solution of 4-isopropenyl-2-methoxy-1-methoxymethoxy-benzene (3.5 g, 16.81 mmol) in 20 mL MeOH, Pd/C (10%, 350 mg) was added and the mixture was stirred 16 h under a H2 atmosphere. The reaction mixture was then filtered through Celite and evaporated in vacuo and briefly dried under vacuum to yield the title compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07319101B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-9268edd1e713488bb67119630f1e5147 |
| Source note | uspto-grants-2008_01 |