HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dichlorophenylboronic acid → 5-(3,5-Dichlorophenyl)-3,3-dimethylindan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dichlorophenylboronic acid | HCID 2734331 | — |
| Reactant | Trifluoromethanesulfonic acid 3,3-dimethyl-1-oxo-indan-5-yl ester | HCID 57618520 | — |
| Product | 5-(3,5-Dichlorophenyl)-3,3-dimethylindan-1-one | HCID 69036350 | — |
Reaction Steps
The title compound was prepared from trifluoro-methanesulfonic acid 3,3-dimethyl-1-oxo-indan-5-yl ester and 3,5-dichlorophenyl boronic acid according to the procedure described in example 21. MS (ES) m/z 305.1; HRMS: calcd for C17H14Cl2O+H+, 305.04944; found (ESI, [M+H]+), 305.0509.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07319152B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-94ce3c6b310c41c9b8623644cf78365f |
| Source note | uspto-grants-2008_01 |