HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Trifluoromethyl)phenylboronic acid → 3,3-Dimethyl-5-[4-(trifluoromethyl)phenyl]indan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Trifluoromethyl)phenylboronic acid | HCID 2734389 | — |
| Reactant | Trifluoromethanesulfonic acid 3,3-dimethyl-1-oxo-indan-5-yl ester | HCID 57618520 | — |
| Product | 3,3-Dimethyl-5-[4-(trifluoromethyl)phenyl]indan-1-one | HCID 69039117 | — |
Reaction Steps
The title compound was prepared from trifluoro-methanesulfonic acid 3,3-dimethyl-1-oxo-indan-5-yl ester and 4-(trifluoromethyl)phenyl boronic acid according to the procedure described in example 21. MS m/z 305; HRMS: calcd for C18H15F3O+H+, 305.11478; found (ESI, [M+H]+), 305.1145.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07319152B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-e9d1cf3b1e8e4dbb9d3550aaf48aaff3 |
| Source note | uspto-grants-2008_01 |