Oxalyl chloride → HCID 54107931, compound

HRID 2251916Notes

Reaction equation

HRID 2251916 reaction equation
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([CH:7]=[CH:8][C:9]([OH:11])=O)[CH:2]=1.C(Cl)(=O)C(Cl)=O.[C:18]1([N:24]([C:35]2[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=2)[C:25](=[O:34])[NH:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][NH2:33])[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>>[C:18]1([N:24]([C:35]2[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=2)[C:25](=[O:34])[NH:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][NH:33][C:9](=[O:11])[CH:8]=[CH:7][C:3]2[CH:2]=[N:1][CH:6]=[CH:5][CH:4]=2)[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=1

Participants

4

Reactant 3

HCID 65578Oxalyl chlorideHCID 1019843-(3-Pyridinyl)-2-propenoic acidHCID 20482959HCID 20482959, compound

Product 1

HCID 54107931HCID 54107931, compound

Procedure

Batch size: 2.6 g (17.6 mmol) 3-(3-pyridyl)-acrylic acid, 1.8 ml (20.8 mmol) oxalyl chloride and 5.0 g (16.0 mmol) 6-(3,3-diphenyl-ureido)-hexylamine.

Sources & evidence

ORD record
ord-a830a8840b7a4bf7aa6e4e127729f846
Source dataset
uspto-grants-2008_01
Patent number
US07320993B1

Reaction notes

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