HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 54355152, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 3-(3-Pyridinyl)-2-propenoic acid | HCID 101984 | — |
| Reactant | HCID 69306792 | HCID 69306792 | — |
| Product | HCID 54355152 | HCID 54355152 | — |
Reaction Steps
Batch size: 2.2 g (14.8 mmol) 3-(3-pyridyl)-acrylic acid, 2.5 g (19.7 mmol) oxalyl chloride, 4.5 g (44.5 mmol) TEA and 5.0 g (13.4 mmol) 6-(10,11-dihydro-dibenzo[b,f]azepin-5-yl-carbonylamino)-hexylamine hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07320993B1 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-f5de9445a6af433e8e76f5ac691a1937 |
| Source note | uspto-grants-2008_01 |