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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2251923Generated: November 3, 2026

Oxalyl chloride → HCID 53635111, compound

https://huagongshe.com/reaction/2251923

Reaction equation

Participants

RoleNameHCIDCharge
ReactantOxalyl chlorideHCID 65578—
Reactant3-(3-Pyridinyl)-2-propenoic acidHCID 101984—
ReactantHCID 17940753HCID 17940753—
ProductHCID 53635111HCID 53635111—

Reaction Steps

Batch size: 4.1 g (27.5 mmol) 3-(3-pyridyl)-acrylic acid, 4.7 g (37.0 mmol) oxalyl chloride, 5.0 g (49.4 mmol) TEA and 8.6 g (25.0 mmol) 6-(tosylamino)-hexylamine.dihydrochloride.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07320993B1
Source datasetuspto-grants-2008_01
ORD IDord-4db86aa3cff14b16b7ee64f4015e276f
Source noteuspto-grants-2008_01