Oxalyl chloride → HCID 54061138, compound

HRID 2251925Notes

Reaction equation

HRID 2251925 reaction equation
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([CH:7]=[CH:8][C:9]([OH:11])=O)[CH:2]=1.C(Cl)(=O)C(Cl)=O.[C:18]1([C:24]2[N:25]=[CH:26][N:27]([CH2:35][CH2:36][CH2:37][CH2:38][NH2:39])[C:28]=2[C:29]2[CH:34]=[CH:33][CH:32]=[CH:31][CH:30]=2)[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>>[C:18]1([C:24]2[N:25]=[CH:26][N:27]([CH2:35][CH2:36][CH2:37][CH2:38][NH:39][C:9](=[O:11])[CH:8]=[CH:7][C:3]3[CH:2]=[N:1][CH:6]=[CH:5][CH:4]=3)[C:28]=2[C:29]2[CH:30]=[CH:31][CH:32]=[CH:33][CH:34]=2)[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=1

Participants

4

Reactant 3

HCID 65578Oxalyl chlorideHCID 1019843-(3-Pyridinyl)-2-propenoic acidHCID 99658394-(4,5-Diphenylimidazol-1-yl)-butylamine

Product 1

HCID 54061138HCID 54061138, compound

Procedure

Batch size: 2.5 g (17.0 mmol) 3-(3-pyridyl)-acrylic acid, 5.9 g (46.3 mmol) oxalyl chloride and 4.5 g (15.4 mmol) 4-(4,5-diphenyl-imidazol-1-yl)-butylamine.

Sources & evidence

ORD record
ord-6fe7abd191274142930b78a8332d5397
Source dataset
uspto-grants-2008_01
Patent number
US07320993B1

Reaction notes

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