HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → N-(5-hydroxy-5,5-diphenyl-pentyl)-3-pyridin-3-yl-acrylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | 3-(3-Pyridinyl)-2-propenoic acid | HCID 101984 | — |
| Reactant | 5-Hydroxy-5,5-diphenyl-pentylamine | HCID 17940742 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | N-(5-hydroxy-5,5-diphenyl-pentyl)-3-pyridin-3-yl-acrylamide | HCID 54276084 | — |
Reaction Steps
Batch size: 1.7 g (11.3 mmol) 3-(3-pyridyl)-acrylic acid, 1.7 g (10 mmol) CDI and 2.4 g (9.4 mmol) 5-hydroxy-5,5-diphenyl-pentylamine in 40 ml abs. THF.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07320993B1 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-dfafbaa946f94283963a6a1ed739b8cf |
| Source note | uspto-grants-2008_01 |