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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2251929Generated: November 2, 2026

1,2-Dichloroethane → HCID 53741205, compound

https://huagongshe.com/reaction/2251929

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,2-DichloroethaneHCID 11—
Reactant1-HydroxybenzotriazoleHCID 75771—
Reactant3-(3-Pyridinyl)-2-propenoic acidHCID 101984—
ReactantHCID 17940766HCID 17940766—
ProductHCID 53741205HCID 53741205—

Reaction Steps

Batch size: 2.0 g (13.4 mmol) 3-(3-pyridyl)-acrylic acid, 3.0 g (29.6 mmol) TEA, 2.4 g (15.6 mmol) 88% HOBT, 3.0 g (15.6 mmol) EDC and 4.0 g (13.4 mmol) 4-diphenylacetylamino-butylamine hydrochloride.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07320993B1
Source datasetuspto-grants-2008_01
ORD IDord-965342c786364787b0f0c7d89d325557
Source noteuspto-grants-2008_01