HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → HCID 54076766, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | 3-(3-Pyridinyl)-2-propenoic acid | HCID 101984 | — |
| Reactant | 4-(Benzhydryl-amino)-butylamine | HCID 12491193 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 54076766 | HCID 54076766 | — |
Reaction Steps
Batch size: 1.9 g (12.6 mmol) 3-(3-pyridyl)-acrylic acid, 2.5 g (15.1 mmol) CDI and 3.7 g (14.5 mmol) 4-(benzhydryl-amino)-butylamine in 60 ml abs. THF.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07320993B1 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-d8e07e6e8d9e457f89bc7a52a3604aa4 |
| Source note | uspto-grants-2008_01 |