Hydrochloric Acid → HCID 17940753, compound

HRID 2251941Notes

Reaction equation

HRID 2251941 reaction equation
C(OC(=O)[NH:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][NH:14][S:15]([C:18]1[CH:24]=[CH:23][C:21]([CH3:22])=[CH:20][CH:19]=1)(=[O:17])=[O:16])(C)(C)C.[ClH:26]>C(O)C>[ClH:26].[ClH:26].[S:15]([NH:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][NH2:7])([C:18]1[CH:19]=[CH:20][C:21]([CH3:22])=[CH:23][CH:24]=1)(=[O:16])=[O:17]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 53714411HCID 53714411, compound

Product 1

HCID 17940753HCID 17940753, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Batch size: 13.0 g (<35 mmol) N-[6-(tosyl-amino)-hexyl]-carbamic acid tert-butyl ester and 7.7 ml (93 mmol) concentrated hydrochloric acid in 100 ml ethanol.

Sources & evidence

ORD record
ord-7a6eaffffe184d4bbebb9287bb184fd4
Source dataset
uspto-grants-2008_01
Patent number
US07320993B1

Reaction notes

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