Hydrazine hydrate (1:1) → HCID 17940760, compound

HRID 2251942Notes

Reaction equation

HRID 2251942 reaction equation
[C:1]1([C:7]([C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=2)=[CH:8][CH2:9][CH2:10][CH2:11][CH2:12][N:13]2C(=O)C3C(=CC=CC=3)C2=O)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.NN.O>C(O)C>[C:24]1([C:7]([C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)=[CH:8][CH2:9][CH2:10][CH2:11][CH2:12][NH2:13])[CH:25]=[CH:26][CH:27]=[CH:28][CH:29]=1

Participants

4

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 17940745HCID 17940745, compound

Product 1

HCID 17940760HCID 17940760, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Batch size: 7.8 g (20. mmol) 2-(6,6-diphenyl-hex-5-enyl)-isoindol-1,3-dione and 2.0 g (40.0 mmol) hydrazine.hydrate in 80 ml ethanol.

Sources & evidence

ORD record
ord-97f75dfcd01b4cd3be556d5a373796af
Source dataset
uspto-grants-2008_01
Patent number
US07320993B1

Reaction notes

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