Hydrochloric Acid → HCID 69306779, compound

HRID 2251945Notes

Reaction equation

HRID 2251945 reaction equation
C(OC(=O)[NH:7][CH2:8][CH2:9][CH2:10][CH2:11][NH:12][C:13]([C@@H:15]1[CH2:17][C@H:16]1[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)=[O:14])(C)(C)C.[ClH:25]>C(O)C>[ClH:25].[C:18]1([C@@H:16]2[CH2:17][C@H:15]2[C:13]([NH:12][CH2:11][CH2:10][CH2:9][CH2:8][NH2:7])=[O:14])[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 53693661HCID 53693661, compound

Product 1

HCID 69306779HCID 69306779, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Batch size: 7.5 g (21.6 mmol) N-[4-(trans-2-phenyl-cyclopro-pyl-carbonylamino)-butyl]-carbamic acid tert-butyl ester and 6.4 ml (77 mmol) concentrated hydrochloric acid in 150 ml ethanol.

Sources & evidence

ORD record
ord-b2e9cc9ae3554269bb838f10537dacfe
Source dataset
uspto-grants-2008_01
Patent number
US07320993B1

Reaction notes

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