Hydrazine hydrate (1:1) → 7-Phenylheptan-1-amine

HRID 2251947Notes

Reaction equation

HRID 2251947 reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][N:14]2C(=O)C3C(=CC=CC=3)C2=O)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.NN.O>C(O)C>[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][NH2:14])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 179407542-(7-Phenyl-heptyl)-isoindol-1,3-dione

Product 1

HCID 64319907-Phenylheptan-1-amine

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Batch size: 11.0 g (34.2 mmol) 2-(7-phenyl-heptyl)-isoindol-1,3-dione and 3.4 g (68.4 mmol) hydrazine.hydrate in 100 ml ethanol.

Sources & evidence

ORD record
ord-b605a74308d947568078c36829d66805
Source dataset
uspto-grants-2008_01
Patent number
US07320993B1

Reaction notes

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