HRID2252053

反应详情

EQUATION

反应方程式

HRID 2252053 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Add 4-hydroxymethyl-N-methyl-benzenesulfonamide (0.28 g) to a mixture of manganese dioxide (2.8 g) in 20 mL of dichloromethane. Stir at room temperature overnight and filter over Celite®. Concentrate under reduced pressure to provide (0.11 g, 40%) of the title compound as oil.

WORKUP

后处理

  1. filtrationfilter over Celite®
  2. concentrationConcentrate under reduced pressure