HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → HCID 69208709, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | HCID 69208744 | HCID 69208744 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 69208709 | HCID 69208709 | 84% |
Reaction Steps
Prepare essentially as described in the previous preparation (Preparation 97) starting from 2-(tert-butyldimethyl-silyloxy)-1-[2-chloro-3-(propane-2-sulfonyl)-3H-benzimidazol-5-yl]-2-phenyl-ethanone (760 mg, 1.50 mmol), ethyl amine (0.25 mL, 4.50 mmol, 3 equiv) in 2 mL of THF. Yield: 84%. MS(ES+): m(z=516.3 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07320995B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-0623393c57df471a8685909d9dbf951b |
| Source note | uspto-grants-2008_01 |