HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 17981752, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 69207373 | HCID 69207373 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 17981752 | HCID 17981752 | 15% |
Reaction Steps
Stir a solution of 1-isopropylsulfonyl-2-amino-6-(1-(4-(N-[tert-butoxycarbonyl]amino)cyclohex-1-yl)-4-(phenyl)-imidazol-5-yl)-benzimidazole (0.14 g, 0.2 mmol) in 1 M hydrogen chloride in acetic acid (5 mL) at room temperature for 1 hour. Filter the suspension and dry the solid to provide 0.017 g (15%) of the title compound. MS(ES+): m/z=479.0 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07320995B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-d66e9d0fe7f1446ca1fdff92d3084a45 |
| Source note | uspto-grants-2008_01 |