HRID225208

反应详情

EQUATION

反应方程式

HRID 225208 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

One gram of 1,4-dimethoxy-9,10-dihydro-9,10-ethanoanthracene-11,12-diol, is suspended in 30 ml. of an aqueous solution containing 0.77 g. of potassium periodate and one ml. of ethanol. After stirring at room temperature for 24 hours the insoluble material is removed by filtration, washed well with water and dried leaving a yellow product, m.p. 129°-132° C.

WORKUP

后处理

  1. additionof an aqueous solution containing 0.77 g
  2. customis removed by filtration
  3. washwashed well with water
  4. customdried
  5. customleaving a yellow product, m.p. 129°-132° C.