Sodium periodate → HCID 23329598, compound

Participants

Reaction Steps

A 2.5 g. portion of cis-2-methyl-9,10-dihydro-9,10-ethanoanthracene-11,12-diol [obtained above as yellow crystals (m.p. 227°-228° C.)] is suspended in 100 ml. of an aqueous solution containing 2.14 g. of sodium periodate and one ml. of ethanol. The mixture is stirred at room temperature for 2 hours and the solid is collected by filtration, washed with water and dried giving the desired product as a pale yellow solid, m.p. 125°-126° C.

Provenance & Evidence